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Information card for entry 4105735
Preview
Coordinates | 4105735.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C24 H40 S4 Si2 U |
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Calculated formula | C24 H40 S4 Si2 U |
SMILES | [c]12([c]3(C)[c]4([c]5([c]61[U]23451789%10(SSC[Si]6(C)C)[c]2([c]7([c]8([c]9([c]2%10C)C)C)C)[Si](C)(C)CSS1)C)C)C |
Title of publication | Insertion, Isomerization, and Cascade Reactivity of the Tethered Silylalkyl Uranium Metallocene (η5-C5Me4SiMe2CH2-κC)2U |
Authors of publication | Nathan A. Siladke; Joseph W. Ziller; William J. Evans |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2011 |
Journal volume | 133 |
Pages of publication | 3507 - 3516 |
a | 19.6639 ± 0.0015 Å |
b | 8.7482 ± 0.0007 Å |
c | 17.194 ± 0.0013 Å |
α | 90° |
β | 108.577 ± 0.0009° |
γ | 90° |
Cell volume | 2803.7 ± 0.4 Å3 |
Cell temperature | 153 ± 2 K |
Ambient diffraction temperature | 153 ± 2 K |
Number of distinct elements | 5 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0181 |
Residual factor for significantly intense reflections | 0.0162 |
Weighted residual factors for significantly intense reflections | 0.0369 |
Weighted residual factors for all reflections included in the refinement | 0.0376 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.094 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4105735.html
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