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Information card for entry 4105762
Preview
Coordinates | 4105762.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C41 H43 B Cl2 F4 N2 |
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Calculated formula | C41 H43 B Cl2 F4 N2 |
Title of publication | Enantioselective Synthesis of Homoallylic Amines through Reactions of (Pinacolato)allylborons with Aryl-, Heteroaryl-, Alkyl-, or Alkene-Substituted Aldimines Catalyzed by Chiral C1-Symmetric NHC-Cu Complexes |
Authors of publication | Erika M. Vieira; Marc L. Snapper; Amir H. Hoveyda |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2011 |
Journal volume | 133 |
Pages of publication | 3332 - 3335 |
a | 9.4246 ± 0.0011 Å |
b | 17.954 ± 0.002 Å |
c | 11.732 ± 0.0014 Å |
α | 90° |
β | 110.801 ± 0.002° |
γ | 90° |
Cell volume | 1855.8 ± 0.4 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 6 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0614 |
Residual factor for significantly intense reflections | 0.0554 |
Weighted residual factors for significantly intense reflections | 0.1518 |
Weighted residual factors for all reflections included in the refinement | 0.1581 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.044 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4105762.html
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