Crystallography Open Database

Information card for entry 4105785

Preview

Coordinates	4105785.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C233 H284 Ag43 N11 O97 P12 V18
Calculated formula	C233 H280 Ag43 N11 O97 P12 V18
Title of publication	Silver(I)-Ethynide Clusters Constructed with Phosphonate-Functionized Polyoxovanadates
Authors of publication	Yun-Peng Xie; Thomas C. W. Mak
Journal of publication	Journal of the American Chemical Society
Year of publication	2011
Journal volume	133
Pages of publication	3760 - 3763
a	23.597 ± 0.007 Å
b	23.139 ± 0.007 Å
c	33.025 ± 0.01 Å
α	90°
β	99.636 ± 0.006°
γ	90°
Cell volume	17778 ± 9 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0791
Residual factor for significantly intense reflections	0.0506
Weighted residual factors for significantly intense reflections	0.1235
Weighted residual factors for all reflections included in the refinement	0.1434
Goodness-of-fit parameter for all reflections included in the refinement	1.067
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4105785.html