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Information card for entry 4105812
Preview
Coordinates | 4105812.cif |
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Original paper (by DOI) | HTML |
Chemical name | Lu{BN2Ar2C2H2}(CH2SiMe3)2(THF)2 |
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Formula | C42 H74 B Lu N2 O2 Si2 |
Calculated formula | C42 H74 B Lu N2 O2 Si2 |
Title of publication | Group 3 and Lanthanide Boryl Compounds: Syntheses, Structures, and Bonding Analyses of Sc-B, Y-B, and Lu-B σ-Coordinated NHC Analogues |
Authors of publication | Liban M. A. Saleh; Krishna Hassomal Birjkumar; Andrey V. Protchenko; Andrew D. Schwarz; Simon Aldridge; Cameron Jones; Nikolas Kaltsoyannis; Philip Mountford |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2011 |
Journal volume | 133 |
Pages of publication | 3836 - 3839 |
a | 10.3787 ± 0.0003 Å |
b | 18.8034 ± 0.0004 Å |
c | 12.3583 ± 0.0003 Å |
α | 90° |
β | 102.152 ± 0.002° |
γ | 90° |
Cell volume | 2357.74 ± 0.1 Å3 |
Cell temperature | 293 K |
Ambient diffraction temperature | 293 K |
Number of distinct elements | 7 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0631 |
Residual factor for significantly intense reflections | 0.0586 |
Weighted residual factors for all reflections | 0.0733 |
Weighted residual factors for significantly intense reflections | 0.0688 |
Weighted residual factors for all reflections included in the refinement | 0.0662 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.061 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4105812.html
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