Information card for entry 4105824

Structure parameters

• Chemical name: bis(mu-3-N,N'-diphenylhydrazido)N,N'diphenylhydrazidobis(mu-phenylamido) tetrakis(tetrahydrofuran)tetramanganese(II)
• Formula: C64 H74 Mn4 N8 O4
• Calculated formula: C64 H74 Mn4 N8 O4
• Title of publication: Synthesis of Tetranuclear, Four-Coordinate Manganese Clusters with "Pinned Butterfly" Geometry Formed by Metal-Mediated N-N Bond Cleavage in Diphenylhydrazine
• Authors of publication: Clifton R. Hamilton; Regina A. Baglia; Alexander D. Gordon; Michael J. Zdilla
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2011
• Journal volume: 133
• Pages of publication: 4208 - 4211
• a: 25.781 ± 0.007 Å
• b: 12.04 ± 0.004 Å
• c: 21.765 ± 0.006 Å
• α: 90°
• β: 118.509 ± 0.017°
• γ: 90°
• Cell volume: 5937 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0435
• Residual factor for significantly intense reflections: 0.0314
• Weighted residual factors for significantly intense reflections: 0.0748
• Weighted residual factors for all reflections included in the refinement: 0.079
• Goodness-of-fit parameter for all reflections included in the refinement: 0.965
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No