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Information card for entry 4105826
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Coordinates | 4105826.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | manganese bis(tms-amide) bis(THF) |
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Chemical name | bis(tetrahydrofuran)bis[bis(trimethylsilylamido)]manganese(II) |
Formula | C20 H52 Mn N2 O2 Si4 |
Calculated formula | C20 H52 Mn N2 O2 Si4 |
SMILES | [Mn](N([Si](C)(C)C)[Si](C)(C)C)(N([Si](C)(C)C)[Si](C)(C)C)([O]1CCCC1)[O]1CCCC1 |
Title of publication | Synthesis of Tetranuclear, Four-Coordinate Manganese Clusters with "Pinned Butterfly" Geometry Formed by Metal-Mediated N-N Bond Cleavage in Diphenylhydrazine |
Authors of publication | Clifton R. Hamilton; Regina A. Baglia; Alexander D. Gordon; Michael J. Zdilla |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2011 |
Journal volume | 133 |
Pages of publication | 4208 - 4211 |
a | 13.8679 ± 0.0019 Å |
b | 12.1188 ± 0.0016 Å |
c | 18.512 ± 0.003 Å |
α | 90° |
β | 97.116 ± 0.002° |
γ | 90° |
Cell volume | 3087.2 ± 0.8 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0458 |
Residual factor for significantly intense reflections | 0.0333 |
Weighted residual factors for significantly intense reflections | 0.0926 |
Weighted residual factors for all reflections included in the refinement | 0.097 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.031 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4105826.html
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Users of the data should acknowledge the original authors of the
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