Crystallography Open Database

Information card for entry 4105876

Preview

Coordinates	4105876.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C41 H89 Co Ge4 Si4
Calculated formula	C41 H89 Co Ge4 Si4
Title of publication	From Tetragermacyclobutene to Tetragermacyclobutadiene Dianion to Tetragermacyclobutadiene Transition Metal Complexes
Authors of publication	Vladimir Ya. Lee; Yuki Ito; Hiroyuki Yasuda; Kazunori Takanashi; Akira Sekiguchi
Journal of publication	Journal of the American Chemical Society
Year of publication	2011
Journal volume	133
Pages of publication	5103 - 5108
a	19.3738 ± 0.0008 Å
b	15.928 ± 0.0006 Å
c	17.0381 ± 0.0007 Å
α	90°
β	90°
γ	90°
Cell volume	5257.7 ± 0.4 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	5
Space group number	56
Hermann-Mauguin space group symbol	P c c n
Hall space group symbol	-P 2ab 2ac
Residual factor for all reflections	0.0326
Residual factor for significantly intense reflections	0.0223
Weighted residual factors for significantly intense reflections	0.0511
Weighted residual factors for all reflections included in the refinement	0.0548
Goodness-of-fit parameter for all reflections included in the refinement	1.042
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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