Information card for entry 4105992

Structure parameters

• Formula: C19 H27 B N O P
• Calculated formula: C19 H27 B N O P
• SMILES: [P@@]([BH3])(N[C@@H]1[C@H](O)Cc2c1cccc2)(C(C)(C)C)c1ccccc1
• Title of publication: Stereoselective Synthesis of P-Stereogenic Aminophosphines: Ring Opening of Bulky Oxazaphospholidines
• Authors of publication: Thierry León; Antoni Riera; Xavier Verdaguer
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2011
• Journal volume: 133
• Pages of publication: 5740 - 5743
• a: 9.8349 ± 0.0006 Å
• b: 13.008 ± 0.0008 Å
• c: 14.6147 ± 0.0011 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1869.7 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0424
• Residual factor for significantly intense reflections: 0.0372
• Weighted residual factors for significantly intense reflections: 0.0945
• Weighted residual factors for all reflections included in the refinement: 0.0979
• Goodness-of-fit parameter for all reflections included in the refinement: 1.107
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No