Information card for entry 4106028

Structure parameters

• Formula: C20 H58 N3 O2 Si6 Yb
• Calculated formula: C20 H58 N3 O2 Si6 Yb
• Title of publication: Synthesis and Stability of Homoleptic Metal(III) Tetramethylaluminates
• Authors of publication: Giovanni Occhipinti; Christian Meermann; H. Martin Dietrich; Rannveig Litlabø; Florian Auras; Karl Wilhelm Törnroos; Cäcilia Maichle-Mössmer; Vidar R. Jensen; Reiner Anwander
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2011
• Journal volume: 133
• Pages of publication: 6323 - 6337
• a: 13.0353 ± 0.0009 Å
• b: 16.0013 ± 0.0007 Å
• c: 16.8519 ± 0.0011 Å
• α: 90°
• β: 92.304 ± 0.005°
• γ: 90°
• Cell volume: 3512.2 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0849
• Residual factor for significantly intense reflections: 0.0612
• Weighted residual factors for significantly intense reflections: 0.0859
• Weighted residual factors for all reflections included in the refinement: 0.0906
• Goodness-of-fit parameter for all reflections included in the refinement: 1.228
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No