Information card for entry 4106225

Structure parameters

• Formula: C112 H164 Cl16 N8 Si6 Zr4
• Calculated formula: C112 H164 Cl16 N8 Si6 Zr4
• Title of publication: Formation of a Donor-Stabilized Tetrasilacyclobutadiene Dication by a Lewis Acid Assisted Reaction of an N-Heterocyclic Chloro Silylene
• Authors of publication: Shigeyoshi Inoue; Jan D. Epping; Elisabeth Irran; Matthias Driess
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2011
• Journal volume: 133
• Pages of publication: 8514 - 8517
• a: 12.428 ± 0.0005 Å
• b: 16.2309 ± 0.0006 Å
• c: 32.2578 ± 0.0014 Å
• α: 90°
• β: 98.835 ± 0.004°
• γ: 90°
• Cell volume: 6429.8 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1184
• Residual factor for significantly intense reflections: 0.0542
• Weighted residual factors for significantly intense reflections: 0.0817
• Weighted residual factors for all reflections included in the refinement: 0.0922
• Goodness-of-fit parameter for all reflections included in the refinement: 0.826
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No