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Information card for entry 4106231
Preview
Coordinates | 4106231.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C17 H15 N O4 |
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Calculated formula | C17 H15 N O4 |
SMILES | O=N(=O)[C@@]1([C@@H](C1)c1ccccc1)C(=O)c1ccc(OC)cc1 |
Title of publication | Asymmetric Rh(II)-Catalyzed Cyclopropanation of Alkenes with Diacceptor Diazo Compounds: p-Methoxyphenyl Ketone as a General Stereoselectivity Controlling Group |
Authors of publication | Vincent N. G. Lindsay; Cyril Nicolas; André B. Charette |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2011 |
Journal volume | 133 |
Pages of publication | 8972 - 8981 |
a | 8.1895 ± 0.0014 Å |
b | 5.7464 ± 0.0009 Å |
c | 16.269 ± 0.003 Å |
α | 90° |
β | 97.801 ± 0.005° |
γ | 90° |
Cell volume | 758.5 ± 0.2 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 4 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0914 |
Residual factor for significantly intense reflections | 0.0535 |
Weighted residual factors for significantly intense reflections | 0.1166 |
Weighted residual factors for all reflections included in the refinement | 0.1303 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.14 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4106231.html
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