Information card for entry 4106278

Structure parameters

• Formula: C23 H21 N Si
• Calculated formula: C23 H21 N Si
• SMILES: c12c(c3c(cccc3)n1c1ccc(cc1)C)c1ccccc1[Si]2(C)C
• Title of publication: Palladium-Catalyzed Synthesis of Benzosilolo[2,3-b]indoles via Cleavage of a C(sp3)-Si Bond and Consequent Intramolecular C(sp2)-Si Coupling
• Authors of publication: Yun Liang; Shaoguang Zhang; Zhenfeng Xi
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2011
• Journal volume: 133
• Pages of publication: 9204 - 9207
• a: 19.804 ± 0.004 Å
• b: 20.045 ± 0.004 Å
• c: 14.952 ± 0.003 Å
• α: 90°
• β: 106.03 ± 0.03°
• γ: 90°
• Cell volume: 5705 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2289
• Residual factor for significantly intense reflections: 0.0472
• Weighted residual factors for significantly intense reflections: 0.0658
• Weighted residual factors for all reflections included in the refinement: 0.0929
• Goodness-of-fit parameter for all reflections included in the refinement: 0.529
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No