Crystallography Open Database

Information card for entry 4106360

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Coordinates	4106360.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C35 H54 Ge N2
Calculated formula	C35 H54 Ge N2
Title of publication	A Neutral, Monomeric Germanium(I) Radical
Authors of publication	William D. Woodul; Emma Carter; Robert Müller; Anne F. Richards; Andreas Stasch; Martin Kaupp; Damien M. Murphy; Matthias Driess; Cameron Jones
Journal of publication	Journal of the American Chemical Society
Year of publication	2011
Journal volume	133
Pages of publication	10074 - 10077
a	10.7845 ± 0.0003 Å
b	21.0658 ± 0.0005 Å
c	28.4655 ± 0.0007 Å
α	90°
β	90°
γ	90°
Cell volume	6466.9 ± 0.3 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	4
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.1707
Residual factor for significantly intense reflections	0.0668
Weighted residual factors for significantly intense reflections	0.1451
Weighted residual factors for all reflections included in the refinement	0.1825
Goodness-of-fit parameter for all reflections included in the refinement	1.013
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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