Information card for entry 4106472

Structure parameters

• Formula: C80 H172 Li2 O8 Si12 U2
• Calculated formula: C80 H148 Li2 O8 Si12 U2
• Title of publication: High-Valent Uranium Alkyls: Evidence for the Formation of UVI(CH2SiMe3)6
• Authors of publication: Skye Fortier; Justin R. Walensky; Guang Wu; Trevor W. Hayton
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2011
• Journal volume: 133
• Pages of publication: 11732 - 11743
• a: 22.313 ± 0.0014 Å
• b: 13.3374 ± 0.0008 Å
• c: 19.3698 ± 0.0012 Å
• α: 90°
• β: 90.352 ± 0.002°
• γ: 90°
• Cell volume: 5764.3 ± 0.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1234
• Residual factor for significantly intense reflections: 0.0456
• Weighted residual factors for significantly intense reflections: 0.1196
• Weighted residual factors for all reflections included in the refinement: 0.1474
• Goodness-of-fit parameter for all reflections included in the refinement: 0.924
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No