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Information card for entry 4106519
Preview
Coordinates | 4106519.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C28 H37.25 N O8.12 |
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Calculated formula | C28 H37.25 N O8.125 |
Title of publication | Application of a New Chiral Phosphepine to the Catalytic Asymmetric Synthesis of Highly Functionalized Cyclopentenes That Bear an Array of Heteroatom-Substituted Quaternary Stereocenters |
Authors of publication | Yuji Fujiwara; Gregory C. Fu |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2011 |
Journal volume | 133 |
Pages of publication | 12293 - 12297 |
a | 12.0044 ± 0.0001 Å |
b | 15.5921 ± 0.0002 Å |
c | 16.7986 ± 0.0002 Å |
α | 65.209 ± 0.001° |
β | 76.525 ± 0.001° |
γ | 89.311 ± 0.001° |
Cell volume | 2762.81 ± 0.06 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 4 |
Space group number | 1 |
Hermann-Mauguin space group symbol | P 1 |
Hall space group symbol | P 1 |
Residual factor for all reflections | 0.0307 |
Residual factor for significantly intense reflections | 0.0304 |
Weighted residual factors for significantly intense reflections | 0.0807 |
Weighted residual factors for all reflections included in the refinement | 0.081 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.039 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4106519.html
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Users of the data should acknowledge the original authors of the
structural data.