Information card for entry 4106743

Structure parameters

• Formula: C73.19 H148.26 Bi6 K4 N9.19 O24 Pd3 Sn8
• Calculated formula: C73.19 H74.38 Bi6 K4 N9.19 O24 Pd3 Sn8
• Title of publication: [Pd3Sn8Bi6]4-: A 14-Vertex Sn/Bi Cluster Embedding a Pd3 Triangle
• Authors of publication: Felicitas Lips; Rodolphe Clérac; Stefanie Dehnen
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2011
• Journal volume: 133
• Pages of publication: 14168 - 14171
• a: 13.825 ± 0.003 Å
• b: 16.323 ± 0.003 Å
• c: 27.335 ± 0.006 Å
• α: 76.22 ± 0.03°
• β: 82.55 ± 0.03°
• γ: 65.9 ± 0.03°
• Cell volume: 5465 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1083
• Residual factor for significantly intense reflections: 0.0772
• Weighted residual factors for significantly intense reflections: 0.1882
• Weighted residual factors for all reflections included in the refinement: 0.2058
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No