Crystallography Open Database

Information card for entry 4106782

Preview

Coordinates	4106782.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C46 H55 B F20 Si5 Sn
Calculated formula	C46 H55 B F20 Si5 Sn
Title of publication	Persistent Dialkyl(silyl)stannylium Ions
Authors of publication	Annemarie Schäfer; Wolfgang Saak; Detlev Haase; Thomas Müller
Journal of publication	Journal of the American Chemical Society
Year of publication	2011
Journal volume	133
Pages of publication	14562 - 14565
a	12.1975 ± 0.0004 Å
b	12.7938 ± 0.0004 Å
c	18.1555 ± 0.0005 Å
α	83.93 ± 0.001°
β	74.371 ± 0.001°
γ	83.488 ± 0.001°
Cell volume	2702.47 ± 0.14 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0429
Residual factor for significantly intense reflections	0.0308
Weighted residual factors for significantly intense reflections	0.0739
Weighted residual factors for all reflections included in the refinement	0.0833
Goodness-of-fit parameter for all reflections included in the refinement	1.067
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4106782.html