Crystallography Open Database

Information card for entry 4107373

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Coordinates	4107373.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H66 B N6 Si2 Tm
Calculated formula	C34 H66 B N6 Si2 Tm
Title of publication	Heteroleptic Tm(II) Complexes: One More Success for Trofimenko's Scorpionates
Authors of publication	Jianhua Cheng; Josef Takats; Michael J. Ferguson; Robert McDonald
Journal of publication	Journal of the American Chemical Society
Year of publication	2008
Journal volume	130
Pages of publication	1544 - 1545
a	16.787 ± 0.002 Å
b	18.042 ± 0.002 Å
c	26.963 ± 0.004 Å
α	90°
β	91.884 ± 0.0018°
γ	90°
Cell volume	8161.9 ± 1.8 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0365
Residual factor for significantly intense reflections	0.0303
Weighted residual factors for significantly intense reflections	0.0652
Weighted residual factors for all reflections included in the refinement	0.068
Goodness-of-fit parameter for all reflections included in the refinement	1.162
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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