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Information card for entry 4107463
Preview
Coordinates | 4107463.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C34 H62 Lu N P2 Si2 |
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Calculated formula | C34 H62 Lu N P2 Si2 |
SMILES | [Lu]12(N(c3c([P]1(C(C)C)C(C)C)cc(cc3)C)c1c([P]2(C(C)C)C(C)C)cc(cc1)C)(C[Si](C)(C)C)C[Si](C)(C)C |
Title of publication | A Lanthanide Phosphinidene Complex: Synthesis, Structure, and Phospha-Wittig Reactivity |
Authors of publication | Jason D. Masuda; Kimberly C. Jantunen; Oleg V. Ozerov; Kevin J. T. Noonan; Derek P. Gates; Brian L. Scott; Jaqueline L. Kiplinger |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2008 |
Journal volume | 130 |
Pages of publication | 2408 - 2409 |
a | 11.8412 ± 0.0016 Å |
b | 12.0344 ± 0.0017 Å |
c | 15.568 ± 0.002 Å |
α | 93.12 ± 0.002° |
β | 109.31 ± 0.001° |
γ | 112.128 ± 0.001° |
Cell volume | 1898.4 ± 0.4 Å3 |
Cell temperature | 141 ± 2 K |
Ambient diffraction temperature | 141 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0575 |
Residual factor for significantly intense reflections | 0.0409 |
Weighted residual factors for significantly intense reflections | 0.0827 |
Weighted residual factors for all reflections included in the refinement | 0.0882 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.967 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4107463.html
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