Information card for entry 4107463

Structure parameters

• Formula: C34 H62 Lu N P2 Si2
• Calculated formula: C34 H62 Lu N P2 Si2
• SMILES: [Lu]12(N(c3c([P]1(C(C)C)C(C)C)cc(cc3)C)c1c([P]2(C(C)C)C(C)C)cc(cc1)C)(C[Si](C)(C)C)C[Si](C)(C)C
• Title of publication: A Lanthanide Phosphinidene Complex: Synthesis, Structure, and Phospha-Wittig Reactivity
• Authors of publication: Jason D. Masuda; Kimberly C. Jantunen; Oleg V. Ozerov; Kevin J. T. Noonan; Derek P. Gates; Brian L. Scott; Jaqueline L. Kiplinger
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2008
• Journal volume: 130
• Pages of publication: 2408 - 2409
• a: 11.8412 ± 0.0016 Å
• b: 12.0344 ± 0.0017 Å
• c: 15.568 ± 0.002 Å
• α: 93.12 ± 0.002°
• β: 109.31 ± 0.001°
• γ: 112.128 ± 0.001°
• Cell volume: 1898.4 ± 0.4 ų
• Cell temperature: 141 ± 2 K
• Ambient diffraction temperature: 141 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0575
• Residual factor for significantly intense reflections: 0.0409
• Weighted residual factors for significantly intense reflections: 0.0827
• Weighted residual factors for all reflections included in the refinement: 0.0882
• Goodness-of-fit parameter for all reflections included in the refinement: 0.967
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No