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Information card for entry 4107600
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Coordinates | 4107600.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | Trisilaindane |
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Chemical name | rac-trans-1-Chloro-1-Phenyl-2,2,3-tris(2',4',6'- triisopropylphenyl)-1,2,3-trisilaindane |
Formula | C75 H115 Cl Si3 |
Calculated formula | C75 H115 Cl Si3 |
Title of publication | Syntheses of Trisila Analogues of Allyl Chlorides and Their Transformations to Chlorocyclotrisilanes, Cyclotrisilanides, and a Trisilaindane |
Authors of publication | Kai Abersfelder; David Scheschkewitz |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2008 |
Journal volume | 130 |
Pages of publication | 4114 - 4121 |
a | 13.3185 ± 0.0008 Å |
b | 15.7123 ± 0.0009 Å |
c | 18.0837 ± 0.0011 Å |
α | 78.6948 ± 0.0014° |
β | 75.7526 ± 0.0013° |
γ | 76.4736 ± 0.0013° |
Cell volume | 3527.4 ± 0.4 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0856 |
Residual factor for significantly intense reflections | 0.0696 |
Weighted residual factors for significantly intense reflections | 0.158 |
Weighted residual factors for all reflections included in the refinement | 0.166 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.107 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4107600.html
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