Information card for entry 4107604

Structure parameters

• Formula: Ge39.56 N16 O118 Si12.44
• Calculated formula: Ge39.564 N16 O118 Si12.436
• Title of publication: An Open-Framework Silicogermanate with 26-Ring Channels Built from Seven-Coordinated (Ge,Si)10(O,OH)28 Clusters
• Authors of publication: Kirsten E. Christensen; Charlotte Bonneau; Mikaela Gustafsson; Lei Shi; Junliang Sun; Jekabs Grins; Kjell Jansson; Isabelle Sbille; Bao-Lian Su; Xiadong Zou
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2008
• Journal volume: 130
• Pages of publication: 3758 - 3759
• a: 34.476 ± 0.003 Å
• b: 19.8768 ± 0.0017 Å
• c: 14.8594 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 10182.7 ± 1.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 63
• Hermann-Mauguin space group symbol: C m c m
• Hall space group symbol: -C 2c 2
• Residual factor for all reflections: 0.0701
• Residual factor for significantly intense reflections: 0.0563
• Weighted residual factors for significantly intense reflections: 0.1496
• Weighted residual factors for all reflections included in the refinement: 0.159
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.907 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No