Crystallography Open Database

Information card for entry 4107705

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Coordinates	4107705.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Cs10 Hf2 O86 Si2 W20
Calculated formula	Cs10.01 Hf2 O86 Si2 W20
Title of publication	Synthesis and Catalysis of Di- and Tetranuclear Metal Sandwich-Type Silicotungstates [(γ-SiW10O36)2M2(μ-OH)2]10- and [(γ-SiW10O36)2M4(μ4-O)(μ-OH)6]8- (M = Zr or Hf)
Authors of publication	Yuji Kikukawa; Syuhei Yamaguchi; Kazutaka Tsuchida; Yoshinao Nakagawa; Kazuhiro Uehara; Kazuya Yamaguchi; Noritaka Mizuno
Journal of publication	Journal of the American Chemical Society
Year of publication	2008
Journal volume	130
Pages of publication	5472 - 5478
a	25.3847 ± 0.0016 Å
b	22.6121 ± 0.0014 Å
c	18.8703 ± 0.0011 Å
α	90°
β	124.046 ± 0.003°
γ	90°
Cell volume	8974.9 ± 1 Å³
Cell temperature	153.1 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for significantly intense reflections	0.0644
Weighted residual factors for all reflections included in the refinement	0.211
Goodness-of-fit parameter for all reflections included in the refinement	1.007
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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