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Information card for entry 4107952
Preview
Coordinates | 4107952.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C30 H43 Y |
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Calculated formula | C30 H43 Y |
SMILES | [Y]123456789([c]%12([c]4([c]3([c]2([c]1%12C)C)C)C)CC1(C(=C(C(=C1C)C)C)C9)C)[c]1([c]5([c]6([c]7([c]81C)C)C)C)C |
Title of publication | Reductive Reactivity of the Organolanthanide Hydrides, [(C5Me5)2LnH]x, Leads to an sa-Allyl Cyclopentadienyl (η5-C5Me4CH2-C5Me4CH2-η3)2- and Trianionic Cyclooctatetraenyl (C8H7)3- Ligands |
Authors of publication | William J. Evans; Benjamin M. Schmiege; Sara E. Lorenz; Kevin A. Miller; Timothy M. Champagne; Joseph W. Ziller; Antonio G. DiPasquale; Arnold L. Rheingold |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2008 |
Journal volume | 130 |
Pages of publication | 8555 - 8563 |
a | 9.2799 ± 0.001 Å |
b | 11.1103 ± 0.0012 Å |
c | 12.6823 ± 0.0014 Å |
α | 83.277 ± 0.002° |
β | 78.81 ± 0.002° |
γ | 83.363 ± 0.002° |
Cell volume | 1268.1 ± 0.2 Å3 |
Cell temperature | 163 ± 2 K |
Ambient diffraction temperature | 163 ± 2 K |
Number of distinct elements | 3 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0304 |
Residual factor for significantly intense reflections | 0.0256 |
Weighted residual factors for significantly intense reflections | 0.0635 |
Weighted residual factors for all reflections included in the refinement | 0.0656 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.058 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4107952.html
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Users of the data should acknowledge the original authors of the
structural data.