Crystallography Open Database

Information card for entry 4107988

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Coordinates	4107988.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H47 B2 F8 N5 Pd6
Calculated formula	C38 H44 B2 F8 N5 Pd6
Title of publication	Reductive Coupling of Metal Triangles in Sandwich Complexes
Authors of publication	Tetsuro Murahashi; Yasuhiro Hashimoto; Koji Chiyoda; Mayu Fujimoto; Tomohito Uemura; Ryou Inoue; Sensuke Ogoshi; Hideo Kurosawa
Journal of publication	Journal of the American Chemical Society
Year of publication	2008
Journal volume	130
Pages of publication	8586 - 8587
a	22.759 ± 0.006 Å
b	18.556 ± 0.005 Å
c	11.696 ± 0.003 Å
α	90°
β	116.826 ± 0.004°
γ	90°
Cell volume	4408 ± 2 Å³
Cell temperature	123.2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for significantly intense reflections	0.0675
Weighted residual factors for all reflections included in the refinement	0.095
Goodness-of-fit parameter for all reflections included in the refinement	2.237
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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