Crystallography Open Database

Information card for entry 4108063

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Coordinates	4108063.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H45 N Rh2
Calculated formula	C40 H45 N Rh2
Title of publication	Divalent Dirhodium Imido Complexes: Formation, Structure, and Alkyne Cycloaddition Reactivity
Authors of publication	Shin Takemoto; Shohei Otsuki; Yasuhiro Hashimoto; Ken Kamikawa; Hiroyuki Matsuzaka
Journal of publication	Journal of the American Chemical Society
Year of publication	2008
Journal volume	130
Pages of publication	8904 - 8905
a	12.763 ± 0.004 Å
b	16.265 ± 0.007 Å
c	16.571 ± 0.006 Å
α	90°
β	92.249 ± 0.012°
γ	90°
Cell volume	3437 ± 2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/a 1
Hall space group symbol	-P 2yab
Residual factor for all reflections	0.1543
Residual factor for significantly intense reflections	0.1013
Weighted residual factors for significantly intense reflections	0.2629
Weighted residual factors for all reflections included in the refinement	0.2837
Goodness-of-fit parameter for all reflections included in the refinement	1.431
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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