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Information card for entry 4108079
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Coordinates | 4108079.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | [W(CO)5]2(AdC(O)P3)Nb(N[Np]Ar)3 (C5H10)0.5 |
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Formula | C62.5 H81 N3 Nb O11 P3 W2 |
Calculated formula | C62.5 H81 N3 Nb O11 P3 W2 |
Title of publication | P2Addition to Terminal Phosphide M\τbP Triple Bonds: A Rational Synthesis of cyclo-P3 Complexes |
Authors of publication | Nicholas A. Piro; Christopher C. Cummins |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2008 |
Journal volume | 130 |
Pages of publication | 9524 - 9535 |
a | 13.9056 ± 0.0012 Å |
b | 21.2534 ± 0.0018 Å |
c | 23.425 ± 0.002 Å |
α | 90° |
β | 106.21 ± 0.001° |
γ | 90° |
Cell volume | 6647.8 ± 1 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0361 |
Residual factor for significantly intense reflections | 0.0243 |
Weighted residual factors for significantly intense reflections | 0.0521 |
Weighted residual factors for all reflections included in the refinement | 0.0575 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.042 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4108079.html
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