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Information card for entry 4108118
Preview
Coordinates | 4108118.cif |
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Original paper (by DOI) | HTML |
Formula | C41 H59 Ge N3 |
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Calculated formula | C41 H59 Ge N3 |
SMILES | [Ge]1(N(C(=CC(=[N]1c1c(cccc1C(C)C)C(C)C)C)C)c1c(cccc1C(C)C)C(C)C)Nc1c(cccc1C(C)C)C(C)C |
Title of publication | A Cyclopentadienide Analogue Containing Divalent Germanium and a Heavy Cyclobutadiene-like Dianion with an Unusual Ge4 Core |
Authors of publication | Wenyuan Wang; Shenglai Yao; Christoph van Wüllen; Matthias Driess |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2008 |
Journal volume | 130 |
Pages of publication | 9640 - 9641 |
a | 9.1129 ± 0.0006 Å |
b | 11.3531 ± 0.0007 Å |
c | 19.0282 ± 0.001 Å |
α | 100.36 ± 0.005° |
β | 101.854 ± 0.005° |
γ | 98.627 ± 0.005° |
Cell volume | 1859.2 ± 0.2 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0853 |
Residual factor for significantly intense reflections | 0.0399 |
Weighted residual factors for significantly intense reflections | 0.0513 |
Weighted residual factors for all reflections included in the refinement | 0.0566 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.785 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4108118.html
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Users of the data should acknowledge the original authors of the
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