Information card for entry 4108292

Structure parameters

• Formula: C66 H119 N3 Os2 P4
• Calculated formula: C66 H119 N3 Os2 P4
• Title of publication: Aromatic Diosmatricyclic Nitrogen-Containing Compounds
• Authors of publication: Miguel A. Esteruelas; Ana B. Masamunt; Montserrat Oliván; Enrique Oñate; Marta Valencia
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2008
• Journal volume: 130
• Pages of publication: 11612 - 11613
• a: 12.063 ± 0.003 Å
• b: 16.999 ± 0.005 Å
• c: 17.374 ± 0.005 Å
• α: 86.623 ± 0.005°
• β: 69.525 ± 0.004°
• γ: 84.738 ± 0.004°
• Cell volume: 3322.2 ± 1.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.072
• Residual factor for significantly intense reflections: 0.0432
• Weighted residual factors for significantly intense reflections: 0.0766
• Weighted residual factors for all reflections included in the refinement: 0.0832
• Goodness-of-fit parameter for all reflections included in the refinement: 0.9
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No