Information card for entry 4108383

Structure parameters

• Formula: C30.5 H58 N Ni P2
• Calculated formula: C30.5 H58 N Ni P2
• Title of publication: η2-Organoazide Complexes of Nickel and Their Conversion to Terminal Imido Complexes via Dinitrogen Extrusion
• Authors of publication: Rory Waterman; Gregory L. Hillhouse
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2008
• Journal volume: 130
• Pages of publication: 12628 - 12629
• a: 19.401 ± 0.003 Å
• b: 16.398 ± 0.002 Å
• c: 20.871 ± 0.003 Å
• α: 90°
• β: 101.635 ± 0.003°
• γ: 90°
• Cell volume: 6503.4 ± 1.6 ų
• Cell temperature: 373 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0688
• Residual factor for significantly intense reflections: 0.0515
• Weighted residual factors for significantly intense reflections: 0.1195
• Weighted residual factors for all reflections included in the refinement: 0.1264
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No