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Information card for entry 4108517
Preview
Coordinates | 4108517.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C33 H54 N3 Ni Si2 |
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Calculated formula | C33 H54 N3 Ni Si2 |
SMILES | [Ni](N([Si](C)(C)C)[Si](C)(C)C)=C1N(c2c(cccc2C(C)C)C(C)C)C=CN1c1c(cccc1C(C)C)C(C)C |
Title of publication | Two-Coordinate d9 Complexes. Synthesis and Oxidation of NHC Nickel(I) Amides |
Authors of publication | Carl A. Laskowski; Gregory L. Hillhouse |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2008 |
Journal volume | 130 |
Pages of publication | 13846 - 13847 |
a | 12.7493 ± 0.0013 Å |
b | 13.6346 ± 0.0014 Å |
c | 21.526 ± 0.002 Å |
α | 90° |
β | 106.44 ± 0.002° |
γ | 90° |
Cell volume | 3588.9 ± 0.6 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0593 |
Residual factor for significantly intense reflections | 0.0501 |
Weighted residual factors for significantly intense reflections | 0.1361 |
Weighted residual factors for all reflections included in the refinement | 0.1408 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.042 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4108517.html
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