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Information card for entry 4108526
Preview
Coordinates | 4108526.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C74 H150 Si16 |
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Calculated formula | C74 H150 Si16 |
Title of publication | Synthesis and Reactions of a Stable 1,2-Diaryl-1,2-dibromodisilene: A Precursor for Substituted Disilenes and a 1,2-Diaryldisilyne |
Authors of publication | Takahiro Sasamori; Koji Hironaka; Yusuke Sugiyama; Nozomi Takagi; Shigeru Nagase; Yoshinobu Hosoi; Yukio Furukawa; Norihiro Tokitoh |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2008 |
Journal volume | 130 |
Pages of publication | 13856 - 13857 |
a | 16.6701 ± 0.0004 Å |
b | 16.6701 ± 0.0004 Å |
c | 33.7498 ± 0.0011 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 9378.8 ± 0.4 Å3 |
Cell temperature | 103 ± 2 K |
Ambient diffraction temperature | 103 ± 2 K |
Number of distinct elements | 3 |
Space group number | 94 |
Hermann-Mauguin space group symbol | P 42 21 2 |
Hall space group symbol | P 4n 2n |
Residual factor for all reflections | 0.1762 |
Residual factor for significantly intense reflections | 0.0723 |
Weighted residual factors for significantly intense reflections | 0.1497 |
Weighted residual factors for all reflections included in the refinement | 0.2028 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.026 |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4108526.html
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