Information card for entry 4108646

Structure parameters

• Formula: H94 K24 O225 P4 W52
• Calculated formula: K14.8 O207.4 P4 W52
• Title of publication: "Bottom-Up" Meets "Top-Down" Assembly in Nanoscale Polyoxometalate Clusters: Self-Assembly of [P4W52O178]24- and Disassembly to [P3W39O134]19-
• Authors of publication: Chullikkattil P. Pradeep; De-Liang Long; Carsten Streb; Leroy Cronin
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2008
• Journal volume: 130
• Pages of publication: 14946 - 14947
• a: 42.907 ± 0.0014 Å
• b: 13.2352 ± 0.0006 Å
• c: 36.6384 ± 0.0016 Å
• α: 90°
• β: 93.304 ± 0.004°
• γ: 90°
• Cell volume: 20771.7 ± 1.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1021
• Residual factor for significantly intense reflections: 0.064
• Weighted residual factors for significantly intense reflections: 0.172
• Weighted residual factors for all reflections included in the refinement: 0.1863
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No