Information card for entry 4108935

Structure parameters

• Formula: C33 H26 N2 O14 Rh2
• Calculated formula: C33 H23 N2 O14 Rh2
• Title of publication: Structural and Magnetic Study of O2 Molecules Arranged along a Channel in a Flexible Single-Crystal Host Family
• Authors of publication: Satoshi Takamizawa; Ei-ichi Nakata; Takamasa Akatsuka; Chihiro Kachi-Terajima; Ryosuke Miyake
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2008
• Journal volume: 130
• Pages of publication: 17882 - 17892
• a: 9.599 ± 0.003 Å
• b: 10.531 ± 0.003 Å
• c: 10.748 ± 0.004 Å
• α: 71.525 ± 0.007°
• β: 63.5 ± 0.005°
• γ: 62.985 ± 0.006°
• Cell volume: 857.3 ± 0.5 ų
• Cell temperature: 70 K
• Ambient diffraction temperature: 70 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1378
• Residual factor for significantly intense reflections: 0.0883
• Weighted residual factors for significantly intense reflections: 0.2135
• Weighted residual factors for all reflections included in the refinement: 0.246
• Goodness-of-fit parameter for all reflections included in the refinement: 1.095
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No