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Information card for entry 4109213
Preview
Coordinates | 4109213.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C38 H42 B9 Cl Os P2 |
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Calculated formula | C38 H42 B9 Cl Os P2 |
SMILES | [OsH]123(Cl)([P](c4ccccc4)(c4ccccc4)c4ccccc4)([P](c4ccccc4)(c4ccccc4)c4ccccc4)[B]456([BH]789[BH]%10%11%12[BH]%13%14%15[BH]%16%17%10[BH]%107%11[BH]%17([CH]%14%16[B]26%15([BH]48%12%13)[H]3)[CH]59%10)[H]1 |
Title of publication | Stable exo-nido-Metallacarboranes (M = OsIV) that Incorporatemeta-Carborane-Based Dicarbollide Ligands |
Authors of publication | Elena V. Balagurova; Dmitri N. Cheredilin; Galina D. Kolomnikova; Oleg L. Tok; Fedor M. Dolgushin; Alexander I. Yanovsky; Igor T. Chizhevsky |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2007 |
Journal volume | 129 |
Pages of publication | 3745 - 3753 |
a | 11.216 ± 0.004 Å |
b | 12.711 ± 0.006 Å |
c | 14.318 ± 0.005 Å |
α | 95.62 ± 0.03° |
β | 106.15 ± 0.03° |
γ | 91.1 ± 0.03° |
Cell volume | 1949 ± 1.4 Å3 |
Cell temperature | 193 ± 2 K |
Ambient diffraction temperature | 193 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0623 |
Residual factor for significantly intense reflections | 0.0391 |
Weighted residual factors for significantly intense reflections | 0.086 |
Weighted residual factors for all reflections included in the refinement | 0.0908 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.02 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4109213.html
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Users of the data should acknowledge the original authors of the
structural data.