Information card for entry 4109245

Structure parameters

• Formula: C69 H57 B F24 N2 Pt
• Calculated formula: C69 H57 B F24 N2 Pt
• Title of publication: Mechanistic Studies of Platinum(II)-Catalyzed Ethylene Dimerization: Determination of Barriers to Migratory Insertion in Diimine Pt(II) Hydrido Ethylene and Ethyl Ethylene Intermediates
• Authors of publication: Masashi Shiotsuki; Peter S. White; Maurice Brookhart; Joseph L. Templeton
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2007
• Journal volume: 129
• Pages of publication: 4058 - 4067
• a: 11.9369 ± 0.0005 Å
• b: 14.9994 ± 0.0005 Å
• c: 18.276 ± 0.0008 Å
• α: 89.172 ± 0.003°
• β: 86.881 ± 0.003°
• γ: 87.947 ± 0.003°
• Cell volume: 3265.1 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0844
• Residual factor for significantly intense reflections: 0.0528
• Weighted residual factors for significantly intense reflections: 0.1284
• Weighted residual factors for all reflections included in the refinement: 0.1473
• Goodness-of-fit parameter for all reflections included in the refinement: 0.972
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No