Information card for entry 4109527

Structure parameters

• Formula: C123 H172 N8 O6 Si4
• Calculated formula: C123 H172 N8 O6 Si4
• Title of publication: An Isolable Silanoic Ester by Oxygenation of a Stable Silylene
• Authors of publication: Shenglai Yao; Yun Xiong; Markus Brym
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2007
• Journal volume: 129
• Pages of publication: 7268 - 7269
• a: 11.627 ± 0.005 Å
• b: 13.155 ± 0.004 Å
• c: 21.083 ± 0.011 Å
• α: 99.44 ± 0.03°
• β: 94.68 ± 0.04°
• γ: 115.22 ± 0.04°
• Cell volume: 2836 ± 2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2156
• Residual factor for significantly intense reflections: 0.0734
• Weighted residual factors for significantly intense reflections: 0.0812
• Weighted residual factors for all reflections included in the refinement: 0.1068
• Goodness-of-fit parameter for all reflections included in the refinement: 0.877
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No