Information card for entry 4109540

Structure parameters

• Formula: C57.5 H69.5 N4.5 Ni2 O9
• Calculated formula: C57.5 H63.5 N4.5 Ni2 O9
• Title of publication: Dynamic Interconversion of Amorphous Microparticles and Crystalline Rods in Salen-Based Homochiral Infinite Coordination Polymers
• Authors of publication: You-Moon Jeon; Jungseok Heo; Chad A. Mirkin
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2007
• Journal volume: 129
• Pages of publication: 7480 - 7481
• a: 13.3754 ± 0.0012 Å
• b: 15.3953 ± 0.0014 Å
• c: 15.7098 ± 0.0015 Å
• α: 70.609 ± 0.002°
• β: 70.501 ± 0.002°
• γ: 67.214 ± 0.002°
• Cell volume: 2733.9 ± 0.4 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 5
• Space group number: 1
• Hermann-Mauguin space group symbol: P 1
• Hall space group symbol: P 1
• Residual factor for all reflections: 0.1351
• Residual factor for significantly intense reflections: 0.0762
• Weighted residual factors for significantly intense reflections: 0.2018
• Weighted residual factors for all reflections included in the refinement: 0.2447
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No