Information card for entry 4109608

Structure parameters

• Formula: C53 H61 F5 P2 Pt Si
• Calculated formula: C53.0015 H61 F5 P2 Pt Si
• Title of publication: sp Carbon Chains Surrounded by sp3 Carbon Double Helices: Directed Syntheses of Wirelike Pt(C\τbC)nPt Moieties That Are Spanned by Two P(CH2)mP Linkages via Alkene Metathesis
• Authors of publication: Laura de Quadras; Eike B. Bauer; Wolfgang Mohr; James C. Bohling; Thomas B. Peters; José Miguel Martín-Alvarez; Frank Hampel; John A. Gladysz
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2007
• Journal volume: 129
• Pages of publication: 8296 - 8309
• a: 11.5289 ± 0.0002 Å
• b: 15.3365 ± 0.0002 Å
• c: 28.3205 ± 0.0003 Å
• α: 84.848 ± 0.001°
• β: 88.311 ± 0.001°
• γ: 85.263 ± 0.001°
• Cell volume: 4968.94 ± 0.12 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0531
• Residual factor for significantly intense reflections: 0.0354
• Weighted residual factors for significantly intense reflections: 0.0886
• Weighted residual factors for all reflections included in the refinement: 0.1059
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No