Information card for entry 4109843

Structure parameters

• Formula: C29 H37.33 N10.67 U1.33
• Calculated formula: C29 H37.3333 N10.6667 U1.33333
• Title of publication: Magnetic Exchange Coupling in Chloride-Bridged 5f-3d Heterometallic Complexes Generated via Insertion into a Uranium(IV) Dimethylpyrazolate Dimer
• Authors of publication: Stosh A. Kozimor; Bart M. Bartlett; Jeffrey D. Rinehart; Jeffrey R. Long
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2007
• Journal volume: 129
• Pages of publication: 10672 - 10674
• a: 11.7663 ± 0.0013 Å
• b: 11.9389 ± 0.0013 Å
• c: 19.363 ± 0.002 Å
• α: 91.531 ± 0.002°
• β: 96.811 ± 0.002°
• γ: 114.129 ± 0.002°
• Cell volume: 2456.4 ± 0.5 ų
• Cell temperature: 160 ± 2 K
• Ambient diffraction temperature: 160 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0759
• Residual factor for significantly intense reflections: 0.0441
• Weighted residual factors for significantly intense reflections: 0.0907
• Weighted residual factors for all reflections included in the refinement: 0.0992
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No