Information card for entry 4110033

Structure parameters

• Formula: C13 H28 Li N Zn
• Calculated formula: C13 H28 Li N Zn
• Title of publication: On the Kinetic and Thermodynamic Reactivity of Lithium Di(alkyl)amidozincate Bases in Directed Ortho Metalation
• Authors of publication: Yoshinori Kondo; James V. Morey; Jacqueline C. Morgan; Hiroshi Naka; Daisuke Nobuto; Paul R. Raithby; Masanobu Uchiyama; Andrew E. H. Wheatley
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2007
• Journal volume: 129
• Pages of publication: 12734 - 12738
• a: 6.769 ± 0.0001 Å
• b: 15.6651 ± 0.0003 Å
• c: 14.3623 ± 0.0003 Å
• α: 90°
• β: 97.6867 ± 0.0008°
• γ: 90°
• Cell volume: 1509.25 ± 0.05 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0335
• Residual factor for significantly intense reflections: 0.0267
• Weighted residual factors for significantly intense reflections: 0.0674
• Weighted residual factors for all reflections included in the refinement: 0.0709
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No