Information card for entry 4110914

Structure parameters

• Common name: 2b anion
• Formula: C72 H164 Li O6 Sb2 Si14
• Calculated formula: C72 H164 Li O6 Sb2 Si14
• Title of publication: One-Electron Reduction of Kinetically Stabilized Dipnictenes: Synthesis of Dipnictene Anion Radicals
• Authors of publication: Takahiro Sasamori; Eiko Mieda; Noriyoshi Nagahora; Kazunobu Sato; Daisuke Shiomi; Takeji Takui; Yoshinobu Hosoi; Yukio Furukawa; Nozomi Takagi; Shigeru Nagase; Norihiro Tokitoh
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2006
• Journal volume: 128
• Pages of publication: 12582 - 12588
• a: 14.8773 ± 0.0002 Å
• b: 25.2561 ± 0.0003 Å
• c: 14.911 ± 0.0002 Å
• α: 90°
• β: 116.56 ± 0.0005°
• γ: 90°
• Cell volume: 5011.42 ± 0.11 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0501
• Residual factor for significantly intense reflections: 0.0415
• Weighted residual factors for significantly intense reflections: 0.1018
• Weighted residual factors for all reflections included in the refinement: 0.1096
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No