Information card for entry 4111016

Structure parameters

• Common name: cis-Pd2(C6H4PPh2)(O2CCF3)2Cl2, 2CH2Cl2
• Formula: C42 H32 Cl6 F6 O4 P2 Pd2
• Calculated formula: C42 H32 Cl6 F6 O4 P2 Pd2
• Title of publication: High Yield Syntheses of Stable, Singly Bonded Pd26+ Compounds
• Authors of publication: F. Albert Cotton; Igor O. Koshevoy; Pascual Lahuerta; Carlos A. Murillo; Mercedes Sanaú; M. Angeles Ubeda; Qinliang Zhao
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2006
• Journal volume: 128
• Pages of publication: 13674 - 13675
• a: 11.4873 ± 0.0009 Å
• b: 12.2811 ± 0.001 Å
• c: 17.4297 ± 0.0014 Å
• α: 96.894 ± 0.001°
• β: 91.521 ± 0.001°
• γ: 111.854 ± 0.001°
• Cell volume: 2258.9 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0555
• Residual factor for significantly intense reflections: 0.0395
• Weighted residual factors for significantly intense reflections: 0.0785
• Weighted residual factors for all reflections included in the refinement: 0.0832
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No