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Information card for entry 4111036
Preview
Coordinates | 4111036.cif |
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Original paper (by DOI) | HTML |
Formula | C118 H160 La4 O8 |
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Calculated formula | C118 H160 La4 O8 |
Title of publication | Trivalent [(C5Me5)2(THF)Ln]2(μ-η2:η2-N2) Complexes as Reducing Agents Including the Reductive Homologation of CO to a Ketene Carboxylate, (μ-η4-O2CCCO)2- |
Authors of publication | William J. Evans; David S. Lee; Joseph W. Ziller; Nikolas Kaltsoyannis |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2006 |
Journal volume | 128 |
Pages of publication | 14176 - 14184 |
a | 14.234 ± 0.006 Å |
b | 14.365 ± 0.006 Å |
c | 15.917 ± 0.007 Å |
α | 91.539 ± 0.007° |
β | 114.067 ± 0.007° |
γ | 109.738 ± 0.007° |
Cell volume | 2745 ± 2 Å3 |
Cell temperature | 163 ± 2 K |
Ambient diffraction temperature | 163 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0877 |
Residual factor for significantly intense reflections | 0.055 |
Weighted residual factors for significantly intense reflections | 0.1374 |
Weighted residual factors for all reflections included in the refinement | 0.1591 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.067 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4111036.html
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