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Information card for entry 4111092
Preview
Coordinates | 4111092.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | 3,3-Bis-trimethylsilyl-1,3-thiasiletane |
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Formula | C8 H22 S Si3 |
Calculated formula | C7.94 H21.82 S Si3 |
Title of publication | Synthesis, Structure, and Chemistry of New, Mixed Group 14 and 16 Heterocycles: Nucleophile-Induced Ring Contraction of Mesocyclic Dications |
Authors of publication | Eric Block; Evgeny V. Dikarev; Richard S. Glass; Jin Jin; Bo Li; Xiaojie Li; Shao-Zhong Zhang |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2006 |
Journal volume | 128 |
Pages of publication | 14949 - 14961 |
a | 12.2325 ± 0.0011 Å |
b | 12.3562 ± 0.0011 Å |
c | 9.6165 ± 0.0009 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1453.5 ± 0.2 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 4 |
Space group number | 60 |
Hermann-Mauguin space group symbol | P b c n |
Hall space group symbol | -P 2n 2ab |
Residual factor for all reflections | 0.0354 |
Residual factor for significantly intense reflections | 0.0334 |
Weighted residual factors for significantly intense reflections | 0.0913 |
Weighted residual factors for all reflections included in the refinement | 0.0936 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.045 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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