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Information card for entry 4111120
Preview
Coordinates | 4111120.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C13 H33 Cl2 N4 P Pd |
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Calculated formula | C13 H33 Cl2 N4 P Pd |
SMILES | [Pd](=CN(C(C)C)C(C)C)([P](N(C)C)(N(C)C)N(C)C)(Cl)Cl |
Title of publication | Cyclic C-Amino Phosphorus Ylides as a Source of Bidentate Heteroditopic Ligands (Phosphine/Aminocarbene) for Transition Metals |
Authors of publication | Joan Vignolle; Bruno Donnadieu; Didier Bourissou; Michèle Soleilhavoup; Guy Bertrand |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2006 |
Journal volume | 128 |
Pages of publication | 14810 - 14811 |
a | 17.7471 ± 0.0012 Å |
b | 8.8609 ± 0.0006 Å |
c | 13.0417 ± 0.0009 Å |
α | 90° |
β | 108.767 ± 0.003° |
γ | 90° |
Cell volume | 1941.8 ± 0.2 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0242 |
Residual factor for significantly intense reflections | 0.0185 |
Weighted residual factors for significantly intense reflections | 0.0453 |
Weighted residual factors for all reflections included in the refinement | 0.0478 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.03 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4111120.html
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Users of the data should acknowledge the original authors of the
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