Information card for entry 4111122

Structure parameters

• Formula: C68 H56 F6 N2 O6 P2 Pd2 S2
• Calculated formula: C68 H56 F6 N2 O6 P2 Pd2 S2
• Title of publication: Cyclic C-Amino Phosphorus Ylides as a Source of Bidentate Heteroditopic Ligands (Phosphine/Aminocarbene) for Transition Metals
• Authors of publication: Joan Vignolle; Bruno Donnadieu; Didier Bourissou; Michèle Soleilhavoup; Guy Bertrand
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2006
• Journal volume: 128
• Pages of publication: 14810 - 14811
• a: 13.0253 ± 0.0004 Å
• b: 14.6703 ± 0.0005 Å
• c: 17.4565 ± 0.0006 Å
• α: 98.194 ± 0.002°
• β: 94.66 ± 0.002°
• γ: 100.156 ± 0.002°
• Cell volume: 3230.46 ± 0.19 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0426
• Residual factor for significantly intense reflections: 0.0313
• Weighted residual factors for significantly intense reflections: 0.0806
• Weighted residual factors for all reflections included in the refinement: 0.0856
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No