Information card for entry 4111378

Structure parameters

• Common name: Cp*2ScSiH(SiMe3)2
• Formula: C26 H49 Sc Si3
• Calculated formula: C26 H42 Sc Si3.004
• Title of publication: Synthesis and Characterization of Scandium Silyl Complexes of the Type Cp*2ScSiHRR'. σ-Bond Metathesis Reactions and Catalytic Dehydrogenative Silation of Hydrocarbons
• Authors of publication: Aaron D. Sadow; T. Don Tilley
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2005
• Journal volume: 127
• Pages of publication: 643 - 656
• a: 9.1426 ± 0.0006 Å
• b: 10.4602 ± 0.0006 Å
• c: 17.096 ± 0.001 Å
• α: 94.074 ± 0.001°
• β: 105.507 ± 0.001°
• γ: 103.56 ± 0.001°
• Cell volume: 1515.83 ± 0.16 ų
• Cell temperature: 132.2 K
• Ambient diffraction temperature: 132.2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0819
• Residual factor for significantly intense reflections: 0.065
• Weighted residual factors for all reflections: 0.0959
• Weighted residual factors for significantly intense reflections: 0.09
• Weighted residual factors for all reflections included in the refinement: 0.09
• Goodness-of-fit parameter for all reflections included in the refinement: 2.39
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No