Information card for entry 4111396

Structure parameters

• Formula: C33 H46 O21
• Calculated formula: C33 H46 O21
• Title of publication: Synthesis of Postulated Molecular Probes: Stereoselective Free-Radical-MediatedC-Glycosylation in Tandem with Hydrogen Transfer
• Authors of publication: Yvan Guindon; Mohammed Bencheqroun; Abderrahim Bouzide
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2005
• Journal volume: 127
• Pages of publication: 554 - 558
• a: 8.841 ± 0.003 Å
• b: 17.598 ± 0.006 Å
• c: 12.876 ± 0.005 Å
• α: 90°
• β: 98.67 ± 0.03°
• γ: 90°
• Cell volume: 1980.4 ± 1.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 3
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0882
• Residual factor for significantly intense reflections: 0.0469
• Weighted residual factors for all reflections: 0.1098
• Weighted residual factors for all reflections included in the refinement: 0.0954
• Goodness-of-fit parameter for all reflections: 0.766
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 1.54056 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No