Information card for entry 4111798

Structure parameters

• Formula: C68 H68 Fe2 Hg O12 P4 Pt Si2
• Calculated formula: C68 H68 Fe2 Hg O12 P4 Pt Si2
• Title of publication: Metal "Capture" by a Heterotrimetalloligand, Heterometallic d10-d10 Interactions, and Unexpected Iron-to-Platinum Silyl Ligand Migration: a Combined Experimental and Theoretical Study
• Authors of publication: Walter Schuh; Pierre Braunstein; Marc Bénard; Marie-Madeleine Rohmer; Richard Welter
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2005
• Journal volume: 127
• Pages of publication: 10250 - 10258
• a: 12.916 ± 0.002 Å
• b: 13.027 ± 0.002 Å
• c: 21.059 ± 0.005 Å
• α: 101.03 ± 0.05°
• β: 100.74 ± 0.05°
• γ: 91.62 ± 0.05°
• Cell volume: 3409.4 ± 1.4 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0547
• Residual factor for significantly intense reflections: 0.036
• Weighted residual factors for significantly intense reflections: 0.0897
• Weighted residual factors for all reflections included in the refinement: 0.0959
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No