Information card for entry 4111862

Structure parameters

• Formula: C35 H51 N3 O4 Si
• Calculated formula: C35 H37 N3 O4 Si
• Title of publication: Total Synthesis of (-)-Spirotryprostatin B: Synthesis and Related Studies
• Authors of publication: Christiane Marti; Erick M. Carreira
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2005
• Journal volume: 127
• Pages of publication: 11505 - 11515
• a: 12.642 ± 0.002 Å
• b: 11.274 ± 0.002 Å
• c: 13.052 ± 0.004 Å
• α: 90°
• β: 104.26 ± 0.02°
• γ: 90°
• Cell volume: 1802.9 ± 0.7 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0598
• Residual factor for significantly intense reflections: 0.0564
• Weighted residual factors for significantly intense reflections: 0.1601
• Weighted residual factors for all reflections included in the refinement: 0.1683
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No